Determination of Deoxynivalenol in Whole Wheat Flour and Whear Bran

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Distribution of deoxynivalenol in wheat, wheat flour, bran, and gluten, and variability associated with the test procedure.

Analytical data obtained on deoxynivalenol (DON) concentration in naturally contaminated wheat during processing in an industrial mill were statistically analyzed, and the distribution functions of DON concentration in lots of wheat, bran, wheat flour, and gluten were estimated. The analytical method had acceptable precision (HORRAT 0.25-0.32) for each test sample. The total variance combined s...

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Gas chromatographic determination of deoxynivalenol in wheat.

Modifications to a published method are described for the determination of deoxynivalenol (DON) in wheat by gas chromatography with electron capture quantitation of the heptafluorobutyrate derivative. In the modified method, DON is extracted by shaking the sample with methanol-water on a wrist-action shaker, followed by filtration through rapid flow paper. One concentration step is eliminated, ...

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ژورنال

عنوان ژورنال: Journal of AOAC INTERNATIONAL

سال: 2002

ISSN: 1060-3271,1944-7922

DOI: 10.1093/jaoac/85.6.1355